CH 223

Chemical Technology Lab - I

0-0-6-6

 

Syllabus:

Identification of unknown organic compounds: element detection, confirmation of the functional groups, derivatization; Separation technique: normal and reduced pressure distillation, solubility method, column chromatography method, sublimation; Isolation of medicinal compounds from plants/other sources: Soxhlet extraction; Preparation: aspirin, paracetamol, imidazole, dye preparation; multistep synthesis; Estimation of organic compounds: paracetamol, glucose; Characterization of unknown organic compounds by UV-Vis, IR and 1H-NMR techniques; Experiment based on polymer science, electrophoresis, protein estimation, catalytic hydrogenation.

Texts and References:

1.     J. R. Mohrig, T. C. Morrill, C. N. Hammond and D.C. Neckers, Experimental organic chemistry, W.H. Freeman and Co. ,1998.

2.     N. K. Vishnoi, Advanced practical organic chemistry, Vikash publishing house Pvt. Ltd. ,1996.

3.     B. S. Furniss, A.J. Hannaford, P.W.G. Smith, and A.R. Tatchell, Vogel's textbooks of practical organic chemistry, 5th Ed., ELBS Longman ,1994.